Translucent γ-AlOOH and γ-Al2O3 glass-ceramics using the cold sintering process
نویسندگان
چکیده
Cold Sintering Process has been applied to hydroxide precursors Al(OH)3, xH2O promote in situ reactive sintering. The application of sintering temperatures < 400°C led the release OH groups and partial crystallization into boehmite γ-AlOOH. This latter step is accompanied by a densification stage leading production dense translucent pellet. From skeletal density measurements, it appears that not all pellet composed crystalline phase, but contains mix amorphous phase. presence phase seems favor mechanical stability samples made intermediate which brittle due its oriented layer structure. Further heat treatment an oven at 500°C induces transformation γ-Al2O3. Here we demonstrate possibility produce optically ceramics low temperature gamma alumina
منابع مشابه
Preparation of translucent YAG:Ce ceramics by reaction sintering
The paper presents preparation of YAG precursor powders mixture with ability for the reaction sintering at lower temperature. The powder mixture was mechanochemically processed and characterized for the specific surface area and crystallinity (XRD). Sintering experiments were performed on the batched powders, mechanochemically processed powders and as-synthesised YAG powders. XRD measurements a...
متن کاملPreparation of γ-Al2O3 and Prioritization of Affecting Factors on the Crystallite Size Using Taguchi Method
In this work, boehmite sol was prepared by a previously applied and validated method; hydrolysis of aluminum chloride hexa-hydrate. In order to obtain precise results, the effect of pH after adding precipitating agent, aging time, peptizing temperature and ultrasonic vibration time on the crystallite size of final precipitate were investigated in a narrow range. The preparation conditions appli...
متن کاملOne-dimensional nanowires of pseudoboehmite (aluminum oxyhydroxide γ-AlOOH).
We report the discovery of a 1D crystalline structure of aluminum oxyhydroxide. It was found in a commercial product of fibrous pseudoboehmite (PB), γ-AlOOH, synthesized easily with low cost. The thinnest fiber found was a ribbon-like structure of only two layers of an Al-O octahedral double sheet having a submicrometer length along its c axis and 0.68-nm thickness along its b axis. This thickn...
متن کاملCold Sintering Process: New sintering technique for fabrication of nano-structured ceramics below 300 °C - A review
Due to the conventional understanding of sintering phenomenon in ceramic materials, considering two words of “cold” and “sintering” together may arise a doubt to a ceramic engineer since the usual sintering process has been accompanied by a heating regime at elevated temperatures. Recently, a new technique called Cold Sintering Process (CSP) has been introduced and developed as an ultra-low tem...
متن کاملProduction of γ-Al2O3 from Kaolin
The paper reports a process for synthesis of γ-alumina from kaolin. Kaolin was transformed to meta-kaolin by calcination at 800 ̊C for 2h. γ-alumina powder was synthesized through extracting alumina from metakaolin via H2SO4 and meta-kaolin reactions and consequently precipitation in ethanol, which led to form the aluminum sulfate. The precipitated aluminum sulfate was dried and calcined at 900 ̊...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Scripta Materialia
سال: 2021
ISSN: ['1359-6462', '1872-8456']
DOI: https://doi.org/10.1016/j.scriptamat.2020.113650